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@ARTICLE{Franke:287629,
author = {V. Franke$^*$ and J. Breitling$^*$ and P. Boyd$^*$ and A.
Feignier$^*$ and R. Bangert$^*$ and N. Weckesser$^*$ and
H.-P. Schlemmer$^*$ and M. Ladd$^*$ and P. Bachert$^*$ and
D. Paech$^*$ and A. Korzowski$^*$},
title = {{A} versatile look-up algorithm for mapping p{H} values and
magnesium ion content using 31 {P} {MRSI}.},
journal = {NMR in biomedicine},
volume = {37},
number = {6},
issn = {0952-3480},
address = {New York, NY},
publisher = {Wiley},
reportid = {DKFZ-2024-00283},
pages = {e5113},
year = {2024},
note = {2024 Jun;37(6):e5113 / #EA:E020#LA:E020#},
abstract = {31 P MRSI allows for the non-invasive mapping of pH and
magnesium ion content (Mg) in vivo, by translating the
chemical shifts of inorganic phosphate and
adenosine-5'-triphosphate (ATP) to pH and Mg via suitable
calibration equations, such as the modified
Henderson-Hasselbalch equation. However, the required
constants in these calibration equations are typically only
determined for physiological conditions, posing a particular
challenge for their application to diseased tissue, where
the biochemical conditions might change manyfold. In this
article, we propose a multi-parametric look-up algorithm
aiming at the condition-independent determination of pH and
Mg by employing multiple quantifiable 31 P spectral
properties simultaneously. To generate entries for an
initial look-up table, measurements from 114 model solutions
prepared with varying chemical properties were made at 9.4
T. The number of look-up table entries was increased by
inter- and extrapolation using a multi-dimensional function
developed based on the Hill equation. The assignment of
biochemical parameters, that is, pH and Mg, is realized
using probability distributions incorporating specific
measurement uncertainties on the quantified spectral
parameters, allowing for an estimation of most plausible
output values. As proof of concept, we applied a version of
the look-up algorithm employing only the chemical shifts of
γ- and β-ATP for the determination of pH and Mg to in vivo
3D 31 P MRSI data acquired at 7 T from (i) the lower leg
muscles of healthy volunteers and (ii) the brains of
patients with glioblastoma. The resulting volumetric maps
showed plausible values for pH and Mg, partly revealing
differences from maps generated using the conventional
calibration equations.},
keywords = {31P MRS (Other) / 31P MRSI (Other) / magnesium (Other) /
magnesium ion concentration (Other) / pH (Other) / pH
imaging (Other)},
cin = {E020 / E010},
ddc = {610},
cid = {I:(DE-He78)E020-20160331 / I:(DE-He78)E010-20160331},
pnm = {315 - Bildgebung und Radioonkologie (POF4-315)},
pid = {G:(DE-HGF)POF4-315},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:38316107},
doi = {10.1002/nbm.5113},
url = {https://inrepo02.dkfz.de/record/287629},
}